1. Locking and Shimming the Sample
2. Routine ¹H and ¹³C Experiments
3. Manual Processing of NMR spectra
4. Automated Procedures
5. Switching between NORMAL and REVERSE Operation
6. Leaving the Spectrometer

B. Advanced 1D Experiments

1. Gated Decoupling (proton coupled carbon spectrum)
2. Inversion Recovery (T1 measurement)
3. DEPT - Experiments / PENDANT
4. Combined DEPT Experiments
5. NOE Difference Spectra
6. Homo-Decoupling Experiments
7. Kinetic ¹H and ¹³C Measurements

C.  2D NMR Experiments:

1. Preparing the 1D Projections
2. Preparing the 2D Experiment
1. H,H COSY
2. H,H NOESY
3. H,H TOCSY
4. J-resolved H,H correlation
5. C,H Correlation
6. COLOC - Long Range C,H Correlation
7. J-resolved C,H Correlation
8. INADEQUATE
3. Processing the 2D Data
4. Plotting the 2D spectra

1. Table 1: Shim Matrix and Job Parameter files for various solvents
2. Table 2: Startup Parameters for the AM-360 NMR Spectrometer
3. 90 Degree Pulse Lengths - AM-360
4. Special Keystrokes
5. Tuning and Matching Settings for the AM 360 - 10 mm BB Probe
6. Emergency Shutdown of the AM-360 spectrometer

 

1. Data Transfer: Spectrometer «--» PC (NMRNET)
2. Using NUTS (Acorn NMR Inc.) to process 1D data
3. Using NUTS (Acorn NMR Inc.) to process 2D data